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Merck

25343

Supelco

SPB®-5 Kapillar-GC-Säule

L × I.D. 30 m × 0.53 mm, df 3.00 μm

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About This Item

UNSPSC-Code:
41115710
eCl@ss:
32119290

Materialien

fused silica

Qualitätsniveau

Agentur

meets requirements for USP G27 and G36

Parameter

-60-260 °C temperature (isothermal)
-60-280 °C temperature (programmed)

Beta-Wert

44

df

3.00 μm

Methode(n)

gas chromatography (GC): suitable

L × ID

30 m × 0.53 mm

Aktive Matrixgruppe

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

Säulenart

capillary non-polar

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Allgemeine Beschreibung

Capillary GC column is also known as open tubular column. The carrier gas flows through the central aperture and is unrestricted throughout the length of the column.
Betriebsbedingungen: Chemisch kompatibel mit Wasser und anderen Injektions- Lösungsmitteln. Empfindlich gegenüber starken anorganischen Säuren und Laugen. Die Säulen können mit Lösungsmitteln gespült werden.

Anwendung

SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. It may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.

Sonstige Hinweise

We offer a variety of chromatography accessories including analytical syringes

Rechtliche Hinweise

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
O Suzuki et al.
Forensic science international, 46(3), 169-180 (1990-07-01)
Positive-ion electron impact (PIEI), positive-ion chemical ionization (PICI) and negative-ion chemical ionization (NICI) mass spectra of 9 carbamate pesticides are presented. In the PIEI mode, the spectra showed small molecular peaks, intense or base peaks due to M - CH3NHCO
Luisito Cercaci et al.
Journal of chromatography. A, 985(1-2), 211-220 (2003-02-13)
The sterol composition of extra virgin olive oil is very characteristic and, thus, has become a helpful tool to detect adulterations with other vegetable oils. Special attention has been addressed to the separate determination of the free and esterified sterol
J M Jurado et al.
Talanta, 106, 14-19 (2013-04-20)
4-Methylsterols and 4,4-dimethylsterols of 47 samples of subcutaneous fat from Iberian pigs reared on two different fattening systems, "Extensive" and "Intensive", have been analyzed by GC-MS and GC-FID. The lipids were extracted by melting the subcutaneous fat in a microwave
Zhihua Fan et al.
Environmental science & technology, 40(19), 6051-6057 (2006-10-21)
A sensitive, simple, and cost-effective passive sampling methodology was developed to quantify personal exposure to gaseous polycyclic aromatic hydrocarbons (PAHs). A Fan-Lioy passive PAH sampler (FL-PPS) is constructed from 320 sections of 1-cm long SPB-5 GC columns (0.75-mm i.d. and

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