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  • Determination of acetamiprid, imidacloprid, and spirotetramat and their relevant metabolites in pistachio using modified QuEChERS combined with liquid chromatography-tandem mass spectrometry.

Determination of acetamiprid, imidacloprid, and spirotetramat and their relevant metabolites in pistachio using modified QuEChERS combined with liquid chromatography-tandem mass spectrometry.

Food chemistry (2017-09-28)
Mohammad Faraji, Roya Noorbakhsh, Hooshang Shafieyan, Mohammadkazem Ramezani
ABSTRACT

A QuEChERS based methodology was developed for the simultaneous identification and quantification of acetamiprid, imidacloprid, and spirotetramat and their relevant metabolites in pistachio by liquid chromatography-tandem mass spectrometry for the first time. First, sample extraction was done with MeCN:citrate buffer:NaHCO

MATERIALS
Product Number
Brand
Product Description

Supelco
Acetamiprid-N-desmethyl, PESTANAL®, analytical standard
Supelco
Supel QuE, Citrate/Sodium Bicarbonate Tube, pk of 50
Supelco
Spirotetramat, PESTANAL®, analytical standard
Supelco
Imidacloprid-d4, PESTANAL®, analytical standard